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Synthesis and characterization of Pb10-xCux(PO4)6O polycrystalline samples

초록

영어

Lee, Kim, et al. reported in July 2023 that a modified lead apatite material, Pb10-xCux(PO4)6O (0.9 < x < 1.1), exhibited superconductivity at room temperature and atmospheric pressure [1, 2]. However, their X-ray diffraction data clearly showed the presence of impurity phases, including Cu2S, raising uncertainty about the sample quality. Subsequent studies have been conducted; however, different samples exhibited various physical properties. To verify the recipe for the sample growth process, we synthesized samples following the methodology outlined in the reference [1, 2]. An analysis of the structure and physical properties of the synthesized sample reaffirms the critical importance of high-quality sample growth.

목차

Abstract
1. INTRODUCTION
2. EXPERIMENTAL
2.1. 원논문 제조법을 활용한 재현성 확인
2.2. 불순물 형성 억제를 위한 제조법 개발 노력
3. RESULT AND DISCUSSION
3.1. 원논문 제조법을 활용한 재현성 확인
3.2. 불순물 형성 억제를 위한 제조법 개발 노력
4. SUMMARY
ACKNOWLEDGMENT
REFERENCES

저자정보

  • Huiwon Kim Department of Physics, Pusan National University, Busan 46241, Korea
  • Minsik Kong Department of Physics, Pusan National University, Busan 46241, Korea
  • Minjae Kim Department of Physics, Pusan National University, Busan 46241, Korea
  • Seohee Kim Department of Physics, Pusan National University, Busan 46241, Korea
  • Jong Mok Ok Department of Physics, Pusan National University, Busan 46241, Korea

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