원문정보
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초록
영어
New 4,4’-[6-(o-carboranylalkoxy)-1,3,5-triazine-2,4-diyl]dimorpholine derivatives have been prepared by reacting 4,4’- [6-(alkynyloxy)-1,3,5-triazine-2,4-diyl]dimorpholines with decaborane and N,N-dimethylaniline as base. The intermediate compounds, 4,4’-[6-(alkynyloxy)-1,3,5-triazine-2,4-diyl]dimorpholines, have been prepared by reacting 4,4’-[6-chloro- 1,3,5-triazine-2,4-diyl]dimorpholines with prop-2-yn-1-ol, but-3-yn-1-ol, and pet-4-yn-1-ol, and potassium tert-butoxide (t- BuOK) as base. The structure of these compounds has been confirmed by IR, 1H, 11B, and 13C NMR and X-ray crystallographic studies.
목차
Abstract
1. Introduction
2. Experimental
2.1. General Considerations
2.2. Synthesis of 4,4’-[6-(Alkynyloxy)-1,3,5-triazine-2,4-diyl]dimorpholine (1).
2.3. Synthesis of 4,4’-[6-(o-Carboranylalkoxy)-1,3,5-triazine-2,4-diyl]dimorpholines (4).
2.5. Crystal Structure Determination
2.6. Supporting Information
3. Results and Discussion
4. Conclusion
References
1. Introduction
2. Experimental
2.1. General Considerations
2.2. Synthesis of 4,4’-[6-(Alkynyloxy)-1,3,5-triazine-2,4-diyl]dimorpholine (1).
2.3. Synthesis of 4,4’-[6-(o-Carboranylalkoxy)-1,3,5-triazine-2,4-diyl]dimorpholines (4).
2.5. Crystal Structure Determination
2.6. Supporting Information
3. Results and Discussion
4. Conclusion
References
저자정보
참고문헌
자료제공 : 네이버학술정보