원문정보
초록
영어
In this work, chemical reduction of various compounds having double, triple bond or aromatic to single bond using a safe continuous flow hydrogenation instrument-H-cube and their physical and chemical property changes are studied. Due to flammability of hydrogen gas, forms an explosion mixture with air and difficulties in work-up has replaced with safe hydrogenation with H-cube having hydrogen generator from electrolysis of water. Here we stabilized the conditions like pressure and temperature for various compounds such as dyes, N-aromatics, chalcone and aliphaticyne compounds. The results obtained from the experiments of this study, in learning the hydrogenation of multiple bonds, will be able to be used as training aids for study of toxic, dye, active drug etc. analysis by physical, chemical and biological changes.
목차
1. INTRODUCTION
2. EXPERIMENTS
2.1. Apparatus
2.2. Reagents
2.3. Methods
2.4. Characterization
3. RESULTS AND DISCUSSION
4. CONCLUSIONS
5. REFERENCES