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논문검색

실험논문(원저논문)

분산제의 첨가가 재활용 지르코니아의 물성에 미치는 영향

원문정보

Effect of addition of dispersant on the physical properties of recycled zirconia

서정일, 박원욱, 김해규

피인용수 : 0(자료제공 : 네이버학술정보)

초록

영어

Purpose: When casting of ceramics, proper amount of deflocculant was added for disperse the particles in slip. In this study, examined the optimum amount of APMA(ammonium polymethaacrylate) water as deflocculant for casting the zirconia. Methods: The 100 g of zirconia powder were ball milled with 300 g zirconia ball, 90 g of distilled water, and APMA water in polyethylene pot for 24 hours. The amount of APMA water were added as deflocculant from 0.5 to 0.9 g at an intervals of 0.1 g. The viscosity of slip with no deflocculant showed 1362c.p. and the minimum viscosity with 580c.p. obtained when the slip contained 0.7% of deflocculant. Bar type specimens were casted with plaster mold and biscuit fired at 1100℃ for 1 hours. Biscuit fired specimens were finished with 60 ㎜(L) × 14 ㎜(W) × 10 ㎜(H) bar. Finished specimens were 2nd fired at 1500℃ for 1 hour. Results: Regardless the addition of deflocculant, all 2nd fired specimens showed 0% of apparent porosity and water absorption. The specimens with no deflocculant showed 24% of drying shrinkage and 27.4% firing shrinkage. On the other hand, The specimens with deflocculant showed 17.4% of drying shrinkage and 17.6% firing shrinkage regardless the amount of deflocculant. The maximum bulk density with 6.09 g/㎤ obtained when the specimens casted with 0.7~0.9% of deflocculant contained slips. Bend strength of specimen with no deflocculant showed 680 ㎫ and the maximum bend strength with 814 MPa obtained when the specimen casted with 0.7% of diflocculant contained slip. Conclusion : It was found that the particle shape of the powder according to the dispersing agent is added, the particle size, sintering temperature and affect the particle size distribution, sintering time, sintering atmosphere, such a great influence on the sintering.

목차

[Abstract]
 I. 서론
 II. 연구 방법
  1. 시편제조
  2. 시험 항목
 III. 결과
  1. 볼밀링한 분체의 미세구조 관찰
  2. 기공률, 흡수율 측정
  3. 건조 수축률 측정
  4. 소성 수축률 측정
  5. 부피비중 측정
  6. 슬립의 점도 측정
  7. 꺾임강도 측정
  8. 미세구조 측정
 IV. 고찰
 V. 결론
 REFERENCES

저자정보

  • 서정일 Jeong-Il Seo. 진주보건대학교 치기공과
  • 박원욱 Won-Uk Park. 진주보건대학교 치기공과
  • 김해규 Hae-Gyu Kim. 진주보건대학교 치기공과

참고문헌

자료제공 : 네이버학술정보

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