원문정보
The Properties of Sintered Body by Using the Slip Casting Process with Remained Dental Zirconia Block after Machining
초록
영어
Purpose: All ceramic crown, made from zirconia instead of metal for core material, is recognized the best esthetical prosthesis. Recently, high-priced zirconia blocks and expensive CAD/CAM machines come into use for making zirconia core. In this study, slip casting process is adapted to evaluate the possibility of the recycling the remained parts of zirconia block after machining. Methods: Remained zirconia blocks were reduced to powders with zirconia mortar, and screened with 180 mesh sieve. Passed powders were ball milled under various conditions to obtain the optimum zirconia slip for casting. Solid casting method was used for casting the specimens with plaster mold. Formed specimens were dried and biscuit fired at 1,000 for 1 hour. Biscuit fired specimens were finished with exact shape of square pillar. Finished specimens were fired from 1,200 to 1,550 at 50 intervals for 1 hour. Linear shrinkage, apparent porosity, water absorption, bulk density, and flexural strength were tested. Microstructures were observed by SEM. Results: Above examinations indicated that the optimum firing temperture was 1,500 , and when fired at this temperature for 1 hour, apparent porosity was 0% and flexural strength was 680 . SEM photomicrographs showed uniform 200~300 grain size, which is equal with microcture of sintered commercial zirconia block. when compare 24% linear shrinkage of cast specimen with 20% linear shrinkage of CAD/CAM machined block, it was estimated that the size controlling of cast core was not so difficult. Conclusion: According to the all of this experimental results, the cast zirconia core produced from the remained parts of zirconia block was possible to use for all ceramic denture.
목차
Ⅰ. 서론
Ⅱ. 연구 방법
1. 제조 공정
2. 시험 항목
Ⅲ. 결과
1. 주입성형을 위한 Ball milling 조건
2. 물성 특성
3. 꺾임 강도
4. Ball milling한 분체의 SEM 관찰
5. 소성한 시편의 SEM 관찰
6. 기존 시편과 폐기물 시편의 물성 비교
Ⅳ. 고찰
Ⅴ. 결론
참고문헌