원문정보
One-pot Synthesis of CdS Nanoparticles by Using Cd(SOCCH3)2Lut2 Precusor and Their Optical Characteristics
초록
영어
A synthetic route for 12 metal thiocarboxylate complex, Cd(SOCCH3)2Lut2 [Lut = 3,5-dimethylpyridine (lutidine)], were investigated for their potential to act as precursors for the formation of cadmium sulfide nanoparticles. Cd(SOCCH3)2Lut2 were characterized by lH-NMR spectroscopy. Thermal decomposition of Cd(SOCCH3)2Lut2 is expected to undergo thiocarboxylic anhydride elimination to give stoichiometric cadmium sulfide nanoparticles and removes the organic supporting ligands cleanly. Prepared cadmium sulfide nanoparticles were characterized by fluorescence and UV-vis absorption spectroscopy and displayed an emission band at 500 nm with an excitation wavelength of 360 nm.
목차
1. 서론
2. 실험
2.1. 일반
2.2. Cd(SOCCH3)2Lut2의 합성
2.3. CdS 나노입자의 합성
2.4. CdS 나노입자의 One-pot 합성
3. 결과 및 고찰
4. 결론
참고문헌