원문정보
Synthesis and Optical Characterization of 1,1-bis(trisilyl)tetraphenylsilole
초록
영어
Silyl-containing tetraphenylsilole, 1,1-bis(trisilyl)tetraphenylsilole, has been synthesized from the reaction of dichlorotetraphenylsilole and dichlorotrisilane and characterized by using NMR spectroscopy. Bis(trisilyl)tetraphenylsilole exhibits an unusual optical property and its optical property was characterized by UV-vis and fluorescence spectroscopy. Absorption wavelength maxima of bis(trisilyl)tetraphenylsilole was 380 nm. Bis(trisilyl)tetraphenylsilole displayed an emission band at 530 nm with an excitation wavelength of 380 nm.
목차
1. 서론
2. 실험
2.1. 일반
2.2. 1,1-Dichlorotetraphenylsilole의 합성[21]
2.3. Chlorodimethyl(phenyl)silane의 합성
2.4. 1,1,2,3,3-Pentamethyl-2-hydro-1,3-diphenyltrisilane의 합성.
2.5. 1,3-Dichlro-1,1,2,3,3-pentaamethyl-2-hydrotrisilane의 합성.
2.6. 1,1-Bis(trisilyl)tetraphenylsilole의 합성
3. 결과 및 고찰
4. 결론
참고문헌