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Research Articles

Simultaneous Determination of Sulfonamides in Porcine and Chicken Muscle Using High Performance Liquid Chromatography with Ultraviolet Detector

원문정보

Yousin Shim, Dongbin Shin, Yongsun Cho, Yunhee Choi, Sanghee Lee

피인용수 : 0(자료제공 : 네이버학술정보)

초록

영어

The present study used the liquid extraction pretreatment method and developed a liquid chromatographyultraviolet detector (LC-UV) for the simultaneous determination of 14 sulfonamides (SAs) residues in porcine and chicken muscle. Linearity within a range of 50-150 μg/kg was obtained with the correlation coefficient (r2) of 0.9673-0.9997. The mean recovery of SAs was 55.9-109.7% (relative standard deviations; RSDs 1.7-17.3%) in porcine muscle and 52.8-112.4% (RSDs 2.3-16.9%) in chicken muscle. The limits of detection (LODs) and limits of quantification (LOQs) were 2-32 and 7-96 μg/kg in porcine muscle, and 4-32 and 13-97 μg/kg in chicken muscle, respectively. These values were lower than the maximum residue limits (MRLs) established by the European Union. The sum of all SAs residues present should be less than 100 μg/kg.

목차

Abstract
 Introduction
 Materials and Methods
 Results and Discussion
 References

저자정보

  • Yousin Shim Korea Food Research Institute
  • Dongbin Shin Korea Food Research Institute
  • Yongsun Cho Korea Food Research Institute
  • Yunhee Choi Korea Food Research Institute
  • Sanghee Lee Korea Food Research Institute

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자료제공 : 네이버학술정보

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